Analysis of the wide-angle neutron scattering of non-graphitic carbon – testing of an advanced evaluation approach

PID

Non-graphitic carbons (NGCs) represent an important class of materials both, in research in industrial applications. A quantitative description of the sp2-polyaromatic microstructure, showing substantial disorder compared to graphite, is desirable for linking material properties to the microstructure. Recently, Ruland and Smarsly introduced a novel approach for the evaluation of the wide-angle X-ray scattering (WAXS) data of non-graphitic carbon, providing meaningful structural parameters describing size and disorder of the graphene stacks. Here we apply for beam time at the E2 instrument to acquire WANS data of six NGC samples for the purpose of further verification of this algorithm and comparison of the structural parameters with those obtained from fitting WAXS data. Compared to WAXS and WANS experiments at FIREPOD, WANS experiments allow for significantly larger values of the modulus of the scattering vector and thus will help to establish the WAXS evaluation as a routine method.

Identifier
PID https://hdl.handle.net/21.11151/zyg1-2wa8
Related Identifier IsCompiledBy https://doi.org/10.5442/NI000001
Metadata Access https://data.helmholtz-berlin.de/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:data.helmholtz-berlin.de:inv/5204
Provenance
Instrument E2 - Flat-Cone Diffractometer,
Publisher Helmholtz-Zentrum Berlin für Materialien und Energie
Contributor Smarsly, Bernd; Pfaff, Torben; Badaczewski, Felix; Loeh, Marc; Helmholtz-Zentrum Berlin für Materialien und Energie
Publication Year 2022
Rights Creative Commons Zero v1.0 Universal; https://creativecommons.org/publicdomain/zero/1.0/
OpenAccess true
Representation
Resource Type Investigation; Collection
Size 268.98 MiB
Discipline Other
Temporal Coverage Begin 2017-04-04T06:00:00Z
Temporal Coverage End 2017-04-12T07:56:26Z