The peculiar hydrogen bonding pattern in crystalline raffinose : a multi-temperature structural study.

DOI

Raffinose is a trisaccharide with a galactose molecule attached to the glucose side of a sucrose moiety. The high similarity with sucrose implies that the presence of raffinose in the crystallization step of sucrose from beet-sugar molasses can severly hamper the process. To shed some light on the interference of raffinose in the crystallization of sucrose, we propose to study its peculiar hydrogen bonding pattern in the crystal, based only on intermolecular interactions, as a function of temperature. Comparing the hydrogen-bonding features in raffinose to those for sucrose, will provide some hints on the solute-solvent interaction and the action mechanism of raffinose as an impurity in the crystallization of sucrose.

Identifier
DOI https://doi.org/10.5286/ISIS.E.63527077
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/63527077
Provenance
Creator Dr Silvia Capelli; Dr Massimo Moret
Publisher ISIS Neutron and Muon Source
Publication Year 2018
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Biology; Biomaterials; Chemistry; Engineering Sciences; Life Sciences; Materials Science; Materials Science and Engineering; Natural Sciences
Temporal Coverage Begin 2015-09-28T09:00:00Z
Temporal Coverage End 2015-10-04T09:00:00Z