Linking the solid state and solution thorium aqua structures: A solid state powder neutron diffraction investigation

DOI

A understanding of the aqueous chemistry of the actinide ions is not as well developed as for transition metals or the lanthanides. Fundamentally important information such as the number of coordinated water molecules is still under debate. This has relied on EXAFS, but this technique cannot give precise coordination numbers. In this work we aim, for the first time, to use neutron diffraction techniques to explicitly locate the coordinated water molecules in three thorium compounds (with bromide, sulfate and chloride ions) of increasing complexity, and understand how these interact with the second coordination shell. In a related submission, we will examine the solution phase structures to gain further information on the structures and stability of these. This information is vital for the storage of spent nuclear fuel either in a geological repository or solution phase processing.

Identifier
DOI https://doi.org/10.5286/ISIS.E.98019456
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/98019456
Provenance
Creator Dr Dominic Fortes; Dr Robert Baker; Mr Samuel Edwards
Publisher ISIS Neutron and Muon Source
Publication Year 2021
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Chemistry; Natural Sciences
Temporal Coverage Begin 2018-09-23T07:00:00Z
Temporal Coverage End 2018-09-25T07:00:00Z