Vibrational spectroscopy on novel N-heterocyclic Pd-catalysts

DOI

We propose to investigate the vibrational dynamics of N-heterocyclic carbenes (NHC) on TOSCA.The here proposed study complements theoretical works in hand for these novel N-heterocyclic carbene (NHC) Pd-catalysts used in alkyl-alkylcross-couplings; it further complements previous neutron spectroscopy studies on TOSCA focusing on the low-energy vibrations/librations of dry and d8-THF solvated pre-catalysts and corresponding ligands. NHC-Pd catalysts show high catalytic activity, out-competing traditional phosphine (ligand) based ones.These systems are largely uncharacterised experimentally from a microscopic point of view. In particular, their reactivities, strongly dependent on ligand alkyl-group substituents (isopropyl, ethyl, methyl); reasoned to be intimately linked to low-energy vibrations and couplings thereof.

Identifier
DOI https://doi.org/10.5286/ISIS.E.24071236
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/24071236
Provenance
Creator Dr Florian Kargl; Dr Gregory Chasse
Publisher ISIS Neutron and Muon Source
Publication Year 2012
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Photon- and Neutron Geosciences
Temporal Coverage Begin 2009-08-07T08:13:16Z
Temporal Coverage End 2009-08-14T12:09:51Z