All primary data files of measurements and processed data of the associated journal article can be found here.
Raw data from physisorption measurements can be found in the dataset of the Traa group.
The data is structured according to experiment type and the material investigated and contains the following data types: PDF, TXT, PDH, GIF, DS8D, GFRM, XLSX
All data was converted to easily readable data types, e.g. TXT. Additional raw data, namely DS8D and GFRM, can be opened with Pyris Software (Perkin Elmer) or SAXS (Bruker AXS), respectively.
General description of filenames:
"Type of Material""massfraction of P123""molar ratio of water to TMOS""time after mixing""unwarped".file extension
Type of Material:
LLC - lyotropic liquid crystal, composed of water and the surfactant P123
LLC-HCl - lyotropic liquid crystal, composed of 0.1 N aqueous HCl solution and the surfactant P123
HM - hybrid material, mixture of water, tetramethyl orthosilicate (TMOS) and P123
MSM - mesoporous silica material, results from the HM after calcination
SBA-15 - commercial mesoporous silica material, no other section of the filename is applicable
P123 - commercial P123, no other section of the filename is applicable
CholPal - commercial cholesteryl palmitate, used for calibration of the sample to detector distance for SAXS experiments in the same folder, no other section of the filename is applicable
AgBeh - commercial silver behenate, used for calibration of the sample to detector distance for WAXS experiments in the same folder, no other section of the filename is applicable
Massfraction of P123:
The massfraction always corresponds to the massfraction in the LLC or LLC parent system.
It is calculated via w(P123) = m(P123)/[m(P123)+m(water)]
The unit is wt.%
Molar ratio of water to TMOS:
This term only applies to HM and MSM.
It is calculated via n(water)/n(TMOS). The value is dimesnionless.
Time after mixing:
This term applies only to the HM and referrs to the reaction time at 80°C after mixing water, TMOS and P123.
Its unit is given with the file name.
Unwarped:
This extension applies to WAXS data only. It indicates a post-meassurement treatment of the data, which takes into accoutn the non-spherical shape of the moveable detector.