Determination of the Interfacial Structure of Lubricating Bottle-Brush Polymer Films at the Steel-Oil Interface

DOI

Lubrication of surfaces by modification with polymer films has proven an efficient method of frictional reduction. Bio-inspired bottle-brush copolymers containing a linear block with surface affinity, and a soluble polymer brush block have shown to be effective lubricants in aqueous systems. We have synthesised bottle-brush copolymers with hydrophilic linear blocks and oil-soluble polymer brushes. These copolymers adsorb to the steel-oil interface leading to a large frictional reduction for oil-based applications. Here, we propose to use polarised neutron reflectometry, exploiting both isotopic and magnetic sensitivity, to determine the structure of bottle-brush copolymer films at the steel-oil interface. This information will allow us to understand the interfacial structure-function relationship of these materials, further directing the design of polymeric lubricants.

Identifier
DOI https://doi.org/10.5286/ISIS.E.RB1920538-1
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/108676620
Provenance
Creator Ms Satu H������kkinen; Dr Paul Kirkman; Miss Jo Searle; Professor Sebastien Perrier; Dr Andrew Kerr; Dr Andrew Caruana; Dr Stephen Hall
Publisher ISIS Neutron and Muon Source
Publication Year 2022
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Chemistry; Natural Sciences
Temporal Coverage Begin 2019-12-16T08:30:00Z
Temporal Coverage End 2019-12-20T14:55:19Z